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Raman System Selection Guide

 
 

Raman System Selection Guide

Raman spectroscopy is quickly becoming one of the preferred chemical identification techniques in many application areas. Raman is advantageous because it is:

Non-invasive: Sample through glass and pastic
Non-destructive: Sample can be reused
Fast: Typical measurement times 5-30 seconds

Raman spectroscopy provides rapid and reliable non-destructive chemical analysis of aqueous solutions, powders, tablets, gels and surfaces. A basic setup consists of a monochromatic source, typically a laser, which interacts with the sample. The scattered radiation is then collected by a spectrometer. We offer several options for using Raman as a measurement tool:

QE65000 Modular Raman System, Click Here

The QE65000 Scientific-grade Spectrometer was designed for low-light level applications such as Raman spectroscopy. You have several grating and entrance aperture sizes from which to choose to optimize a system for your specific application. In

Raman System Selection Guide

addition, we have lasers and Raman probes to complete your own modular Raman setup.

Turnkey Raman Systems, Click Here

We offer several Raman turnkey sensing systems from our partner, Raman Systems, Inc. Their high-performance systems are designed specifically for quick material identification and verification in almost any setting.

PinPointer
 
Pinpointer, the "Point-Click" solution designed specifically for quick material identification and verification on the go and for various field deployments.
PeakSeeker
 
The PeakSeeker by Raman Systems is our most practical and easy-to-use Raman spectrometer. It is an excellent choice for users who want a full featured Raman spectrometer but have a limited budget.
PeakSeeker Pro
 
The PeakSeeker Pro represents the state-of-the-art for an accurate, cost-effective and easy-to-use Raman spectrometer. The premier instrument in the Raman Systems line utilizes TE-cooled, high efficiency CCD detector arrays, and is available with either a 532 nm or 785 nm laser.
RAM-LR Laser
 
A stabilized diode laser (at 785 nm) provides an ideal narrow linewidth excitation source for Raman spectroscopy using CCD detectors. The laser can be controlled through software and has all the laser Class IIIb safety features.
RSM Microscope
 
The Raman Systems RSM Video Raman Microscope is an upright laboratory microscope that couples to a Raman Systems spectrometer (sold separately). The accessory is supplied with a Reflected Light Illuminator and a USB Color Video Camera.
MSK Microscopy Kit
 
The MSK Raman Microscopy Kit from Raman Systems turns an upright laboratory microscope into a video Raman spectroscope. The kit includes a Raman Beamsplitter Module that mounts below the eyepiece assembly and a USB Color Video Camera that mounts above the eyepiece.

 

MMS-Raman, Click Here

Centice Corporation offers their Multimodal Multiplex Spectroscopy Raman System to provide high performance chemical analysis for a fraction of the cost of research-grade systems. Due to its high sensitivity and great resolution, the MMS-Raman is an ideal system for substance verification and accurate concentration analysis, as well as for analysis of very low-concentration samples.

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 


 

Raman Application Areas

Raman spectroscopy is useful for analyzing molecules without a permanent dipole moment, which does not show up on an IR spectrum. Raman spectroscopy is used to determine bond lengths in non-polar molecules. It is useful for determining the identity of organic and inorganic species in solution, as the Raman transitions for these species are more characteristic than for IR, where the transitions are much more affected by the other species present in the solution. Raman can be used to analyze solid, liquid and gaseous sample components even through glass and plastic containers.

Art: Pigments, inks, substrates, resins
Biology: in vivo studies, surface studies, SERS
Catalysts: NO decomposition, kinetics of hydrogenation reactions
Corrosion: corrosion kinetic studies, bronze, aluminum
Forensics: drugs, explosives, pigments, powders, tablets, gels and surfaces, chemicals
Materials: diamond films, semiconductors, nanotubes, asbestos, materials ID
Pharmaceuticals: in situ crystal growth monitoring, kinetics, active ingredients, polymorphs differentiation
Polymers: polymerization monitoring, plasticizer studies, density mapping of films
Process: online monitoring, quality control, research
Other: gemology, geology, chemical and petrochemical processes, water-quality analysis
 
 

 

 

 

 

 

 

 

 

 

 

 

 

 

 


Next-generation Raman Spectroscopy

We've teamed with Centice Corporation to offer next-generation Raman spectroscopy that combines the simplicity of dispersive instruments with the multiplex advantage of a transform spectrometer. The MMS-Raman Spectrometer uses Centice's patent-pending Multimodal Multiplex Spectroscopy to provide high-performance Raman analysis for a fraction of the cost of research-grade systems. The MMS-Raman Spectrometer offers a unique combination of resolving power, spectral range and flexibility, making it an ideal system for the routine analysis of many types of liquids and solids.

How Multimodal Multiplex Spectroscopy Works

Dispersive, fixed-grating spectrometer designs typically use a slit or a fiber as the input into the spectrometer. These apertures restrict the amount of light that can reach the detector. In these designs, there is an inherent tradeoff between resolution and light throughput. While spectral resolution increases as slit width decreases, a narrow input slit limits the light throughput and, likewise, measurement sensitivity. In the MMS-Raman Spectrometer, a wide-area coded aperture takes the place of a traditional slit entrance that allows 10-1000x greater light throughput -- and then applies precise algorithms to extract a high resolution spectrum from the collected light. There is much more light collected, without sacrificing resolution. Multimodal Multiplex Spectroscopy instruments are ideal for measuring weak, scattering and diffuse samples because the spectrometer can collect and process far more light through its wide-area aperture, without affecting spectral resolution.

Key Applications

Key applications include material inspection, identification of unknown materials, and quantitative analysis of both intermediates and final products in the chemical and pharmaceutical industries. Typical samples include powders, liquids and polymers. All experimental and parameter set-up options are computer-controlled for increased ease of use, reliability and speed.

Integrated Sample Holder

The MMS-Raman Spectrometer has a sample holder with cover for operation in full ambient light without affecting performance. The spectrometer's removable sample compartment is integrated into the optical path, avoiding inefficiencies associated with remote compartments. Sample positioning is rapid and precise using the external z-axis alignment control knob. The sample compartment is especially useful for measuring measure weak, scattering and diffuse sources with the highest possible sensitivity. The sample holder supports up to 10-mm cuvettes and test tubes.

MMS-Raman Delivers Great Sensitivity & Resolution

The MMS-Raman spectrometer samples up to 1,000 optical channels simultaneously through the large coded aperture. A mathematical transformation algorithm precisely reconstructs the spectrum with a 4x signal-to-noise improvement as compared with a slit-based system equipped with identical source, grating and detector components, and 70-80x greater than with a fiber input of equivalent resolution.

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

Specification

 

SYSTEM
Wavelength range: 220 cm-1 to 2000 cm-1
Spectral resolution: ~4 cm-1
Grating: Transmissive
Stray light: <0.1%
Integration time: 50 ms to 100 seconds
A/D resolution: 16-bit
APERTURE AND DETECTOR
MMS aperture size: 0.58 mm x 2.3 mm
Detector array size: 512 x 122 pixels
Number of active pixels: 62,464
Pixel size: 24 μm x 24 μm
Well depth: ~300,000 electrons
Quantum efficiency: 85% at 250 nm
Dark noise: 300 e-/pixel/sec @ 0° C
Readout noise: 2 RMS counts, 8 RMS electrons
Gain: 4.7
Detector temperature: To -20 °C below ambient
LASER
Excitation wavelength: 785 nm
Laser power: 70 mW at sample
SAMPLE CHAMBER
Cuvettes: Square, up to 10 mm
Test tubes: Up to 17 mm
COMPUTER
Interface: USB 2.0
Operating systems: Windows XP (with SP2)
RAM requirements: 12 MB

 


 

 

 

 

 
 

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